Week 1: Molecular modeling and Safety: Go over MM, Safety and prepare ethanol sample
SAFETY: Safety Link, Click "view online" or order the book to answer the questions in the safety quiz below Safety Quiz due at the beginning of your next lab (week of Sept 8), hand in bubble sheet How to interpret a MSDS Distillation Prelab due at the beginning of your next lab (week of Sept 15), hand in bubble sheet
MOLECULAR MODELING: MM worksheet due by Friday, Sept 12, in class.
Week 2: No lab Memorial Day
Week 3: Theory of Distillation - meet in prelab
room
Start Fermentation - Bring distillation lab reportSafety Quiz Due at the beginning of prelab
DVD: Distilleries
Week 4: Fractional Distillation Distillation Prelab Due at the beginning of prelab
Procedure: To be handed out - meet in prelab
room first
MM Worksheet Due by Friday, Sept 12. Distillation Lab ReportDue before leaving Mass Spectroscopy Prelab due at the beginning of your next lab
Week 5: Dry lab: UNMC trip Limits of Molecular Modeling - Use Spartan '06 Due Oct 3 use time wisely this week! Stereochemistry Molecular Modeling use Spartan '06 Due Oct 16
Week 6: Mass Spectroscopy: Turn in MS-Prelab. Dry lab - to be done during lab. Steam Distillation Prelab due at the beginning of next lab Cinnamic Acids essay for the prelab.
Week 7: Steam Distillation of Cloves
Procedure: To be handed out
Steam Distillation Prelab Due Lab Report: Report due at start of next lab Limits of
Molecular Modeling Due Oct 3
Stereochemistry Due Oct 16 Chromatography/Extraction Prelab - bring to prelab, to be completed during prelab, collected at the end of prelab
Week 8 Column Chromatography; extraction of chlorophyll and B-carotene Lab report - 2 week lab report, due in two weeks Week 9 Thin Layer chromatography: TLC, and IR Analysis.
J. chem Ed. article - read Lab report - same as last weeks
Week 10 Two Week Extraction, Chromatography, GC/MS and IR data Procedure: Due to Dr. Peitz well before the start of week 12 lab
Your Final Lab report for this lab: Due before the end of the semseter Explosives An application of Molecular Modeling. Use Spartan '06 Due Nov 25 before break.
Week 11 Polarimetry and IR Lab Polarimetry Prelab
Procedure: to be handed out, bring prelab and
report to lab Lab Report: Report due before you leave
Week 12 Conduct week 10 lab that you designed and had verified by Dr. Peitz
Week 13 Mid term Break
Week 14 Fall Break
Week 15 ACS
Week 12 Eugenol SN2 reaction
Procedure
Lab report, GC/MS, class variations, IR
Microbiology data analysis
Organic 315 Chemistry Labs Just like the VCR destroyed the movie industry, the audio
tape destroyed
the music industry, and the photocopier destroyed the print
industry...
Week 3 Synthesis: Esterification of Eugenol Lab Procedure
Lab Report to include IR and GC/MS - Example lab report - available only after you have turned in your report.
Week 6 Diels Alder, Pt. 2 and 13C NMR dry lab
Work on lab report Lab Report to include IR and GC/MS
Prelab Molecular Modeling for Hydrolysis
Week 7 In Lab: Hydrolysis Lab Procedure
Lab Report to include IR and GC/MS
Week 8 Hydrolysis Pt. 2 and 1H NMR dry lab Work on lab
report Lab Report to include IR and GC/MS
Prelab: Molecular Modeling for FC
Week 9 In Lab Friedel Crafts Use the following literature in your G: drive
course_materials 2008_spring_che_031501_organic_chemistry_ii
or che_031502 folder
to help in the development of a full and complete
procedure for the Friedel-Crafts alkylation of Eugenol. Your
text is good too.
1. An AlCl3 Procedure using a different chloride and arene, but similar overall: with-AlCl3.pdf
2. The idea: Student-Designed Experimental Procedure: Student-inquiry.pdf
3. Wikipedia: http://en.wikipedia.org/wiki/Friedel-Crafts_reaction
4. Some MS analysis ideas: GC-MS.pdf
Want to try an acceptable, alternate, green procedure? use the following papers on the G: drive
5. green.pdf
6. green2.pdf